ethanol in not given
react. of borane-THF with 1 equiv. of EtOH;
参考文献
Itsuno, Shinichi; Wakasugi, Takashi; Ito, Koichi; Hirao, Akira; Nakahama, Seiichi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 6 p. 1669 - 1673
byproducts: THF; from -196°C to 0°C, 6 h stirred at 0°C; volatiles destilled out at 0°C, chromatographed on silica-gel in CHCl3, vacuum sublimation at 78°C, vacuum fractional destillation at 70°C;
参考文献
Hosmane, Narayan S.; Sirmokadam, Narayan N.; Mollenhauser, Mark N.
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 359 - 372