4-氯-N，N-二甲基苯甲酰胺合成路线 （共 33 条）
反应条件
in water; ethyl acetate T=20°C; 1 h;
参考文献
Tan, Bin; Toda, Narihiro; Barbas III, Carlos F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12538 - 12541
Angew. Chem., 2012 , vol. 124, # 50 p. 12706 - 12709,4
反应条件
1,1'-carbonyldiimidazole T=160 - 165°C; 1 h;
参考文献
Aavula, Sanjeev Kumar; Chikkulapally, Anil; Hanumanthappa; Jyothi, Indira; Vinod; Sulur, Kumar; Manjunatha; Sythana, Suresh Kumar
Journal of Chemical Research, 2013 , vol. 37, # 3 p. 155 - 159
反应条件
T=270 - 280°C; P=0.7 Torr;
参考文献
Schroth, Werner; Krieg, Reimar; Kluge, Helmut; Gaebler, Michael
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 11 p. 398 - 399
反应条件
methanesulfonic acid; phosphorous pentoxide T=70 - 90°C; 8 h;
参考文献
Kaboudin, Babak; Haghighat, Hamideh
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 951 - 955
反应条件
methanesulfonic acid; phosphorous pentoxide T=70 - 90°C; 8 h;
参考文献
Kaboudin, Babak; Haghighat, Hamideh
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 951 - 955
参考文献
Gupton, John T.; Idoux, John P; Baker, Graeme; Colon, Cesar; Crews, A.Donald; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2933 - 2936
反应条件
amination; 1.5 h; Heating;
参考文献
Woo Song Lee; Ki Hun Park; Yoon
Synthetic Communications, 2000 , vol. 30, # 23 p. 4241 - 4245
反应条件
1: tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide / ethyl acetate / 12 h / 20 - 70 °C 2: ethyl acetate; water / 1 h / 20 °C View Scheme
参考文献
Tan, Bin; Toda, Narihiro; Barbas III, Carlos F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12538 - 12541
Angew. Chem., 2012 , vol. 124, # 50 p. 12706 - 12709,4
反应条件
1: SOCl2 2: (i) THF, (ii) (heating) View Scheme
参考文献
Motoki,S.; Kagami,H.
Journal of Organic Chemistry, 1976 , vol. 41, p. 2759 - 2762
反应条件
hydrogenchloride Yield given;
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
