5,10,15,20-四苯基-21H,23H-卟吩锌合成路线 （共 32 条）
反应条件
zinc diacetate in methanol; chloroform 1 h;
参考文献
He, Chao; He, Qingguo; Deng, Changmin; Shi, Liqi; Zhu, Defeng; Fu, Yanyan; Cao, Huimin; Cheng, Jiangong
Chemical Communications, 2010 , vol. 46, # 40 p. 7536 - 7538
反应条件
in methanol; chloroform tetraphenylporphyrin (300 mg) and Zn(OAc)2*2H2O (800 mg) refluxed (1 h) in CHCl3/MeOH (2:1); cooled; solvent removed (vac.); dissolved in CHCl3; chromd. (silica, CHCl3);
参考文献
Vail, Sean A.; Schuster, David I.; Guldi, Dirk M.; Isosomppi, Marja; Tkachenko, Nikolai; Lemmetyinen, Helge; Palkar, Amit; Echegoyen, Luis; Chen, Xihua; Zhang, John Z. H.
Journal of Physical Chemistry B, 2006 , vol. 110, # 29 p. 14155 - 14166
反应条件
Zn in dimethyl sulfoxide (N2), Zn mediated (50 equiv.) cyclization in DMSO at 85°C for 10 min;
参考文献
Chemical Communications, , # 39 p. 4982 - 4984
反应条件
1: benzaldehyde With zinc diacetate; benzoic acid T=200°C; P=2736.18 Torr; 0.0833333 h; 2: pyrrole T=200°C; 0.333333 h;
参考文献
Nia, Shabnam; Gong, Xianchang; Drain, Charles Michael; Jurow, Matthew; Rizvi, Waqar; Qureshy, Meroz
Journal of Porphyrins and Phthalocyanines, 2010 , vol. 14, # 7 p. 621 - 629
反应条件
in N,N-dimethyl-formamide boiling (excess zinc acetate);
参考文献
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, , vol. 24, # 11 p. 797 - 801
反应条件
in N,N-dimethyl-formamide refluxing; purified by chromy. on silica (silica gel 60) with chloroform, purity >99percent;
参考文献
Journal of Physical Chemistry A, , vol. 105, # 41 p. 9498 - 9508
反应条件
in methanol; dichloromethane; water phorphyrin was dissolved in CH2Cl2 and 1.2 equiv of Zn(OCOCH3)2*H2O in CH3OH:H2O (10:1) were added, the mixt. was stirred for 2 h; washed with water, pptd. with CH3OH;
参考文献
Ventura, Barbara; Flamigni, Lucia; Marconi, Giancarlo; Lodato, Fabio; Officer, David L.
New Journal of Chemistry, 2008 , vol. 32, # 1 p. 166 - 178
反应条件
2,6-dimethylpyridine in tetrahydrofuran Ar atmosphere; stirring (40°C, 30 min); solvent evapn., dissolving (toluene), silica-gel column, washing (toluene, then CH2Cl2/acetone = 50/1 v/v), recrystn. (MeOH/H2O); elem. anal.;
参考文献
Tsukahara, Keiichi; Sawai, Naoko; Hamada, Satoko; Nakazawa, Takashi; Nakagaki, Ryoichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 1947 - 1954
反应条件
in neat (no solvent) byproducts: H2; Zn atoms deposited on Ag(111) surface and then monolayer of H2TPP deposited, heated to 550 K; XPS;
参考文献
Chemical Communications, , # 6 p. 568 - 570
反应条件
1: propionic acid / 1 h / Reflux 2: N,N-dimethyl-formamide / 0.33 h / Reflux View Scheme
参考文献
Journal of Porphyrins and Phthalocyanines, , vol. 16, # 3 p. 267 - 272
