顺-3,7-二甲基-2,6-辛二烯-1-醇乙酸酯合成路线 (共 54 条)
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 1899 - 1902
反应条件
titanium tetrachloride 3.3 h; Heating;
参考文献
Iranpoor, Nasser; Zeynizadeh, Behzad
Synthetic Communications, 1999 , vol. 29, # 12 p. 2123 - 2128
反应条件
sodium acetate in methoxybenzene P=760.051 Torr; 18 h; Heating / reflux; Product distribution / selectivity;
参考文献
WO2005/44774 A1, ;
Page/Page column 16-17 ;
反应条件
1,1-dimethyl-1-(4-methylcyclohex-3-enyl)methanol; sulfur dioxide; water T=40°C; 96 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 21, p. 1331 - 1334
反应条件
acetic anhydride T=80°C; 15 h;
参考文献
Tetrahedron Letters, , vol. 32, # 47 p. 6965 - 6968
反应条件
1: pyridinium p-toluenesulfonate / tetrahydrofuran / Ambient temperature 2: 90 percent / acetic anhydride / 6 h / Heating View Scheme
参考文献
Chemistry Letters, , p. 879 - 882
反应条件
1: 73 percent / NaI , anhydrous NaOAc, zinc powder / acetic acid / 1.5 h 2: 1.) Li / 2.) ether / pet. ether , 10 min , -20 deg C 3: 96 percent / KOH / methanol 4: 50 percent / ethanol / 4 h / Heating 5: 1.) NaI , NaOAc , 2.) SnCl2 , POCl3 / 1.) Propionic acid , AcOH , 30 min , 2.) pyridine , 10 + 60 min , RT View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. <B> 20, # 4 p. 340 - 342