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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丙烯酸丁酯
合成路线
（共 294 条）
141-32-2
丙烯酸丁酯
+
14752-66-0
对氯苯亚磺酸钠
→
反应条件
42175-12-2
反应条件
copper diacetate; palladium diacetate in tetrahydrofuran; dimethyl sulfoxide T=70°C; Heck Reaction; 6 h; stereoselective reaction;
参考文献
Hu, Sai; Xia, Ping; Cheng, Kai; Qi, Chenze
Applied Organometallic Chemistry, 2013 , vol. 27, # 3 p. 188 - 190
1073-67-2
4-氯苯乙烯
+
141-32-2
丙烯酸丁酯
→
反应条件
42175-12-2
反应条件
lithium chloride; [Rh(C2H4)2Cl]2 in xylene Mizoroki-Heck reaction; 12 h; Heating; Title compound not separated from byproducts;
参考文献
Sugihara, Toru; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1765 - 1772
141-32-2
丙烯酸丁酯
+
108-90-7
氯苯
→
反应条件
42175-12-2
+
107776-17-0
+
131061-13-7
反应条件
8-acetamidoquinoline; copper diacetate; palladium diacetate T=120°C; Heck Reaction; 15 h; Overall yield = 84 percent; regioselective reaction;
参考文献
Ying, Cheng-Hao; Yan, Shao-Bai; Duan, Wei-Liang
Organic Letters, 2014 , vol. 16, # 2 p. 500 - 503
141-32-2
丙烯酸丁酯
+
108-90-7
氯苯
→
反应条件
42175-12-2
+
131061-13-7
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; copper (II) acetate monohydrate; trichloroacetic acid T=120°C; 22 h; regioselective reaction;
参考文献
Zheng, Lu; Wang, Jianhui
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9699 - 9704
50-00-0
甲醛
+
141-32-2
丙烯酸丁酯
+
56-40-6
甘氨酸
→
反应条件
122079-54-3
N-丁基吡咯烷-3-羧酸
反应条件
in toluene 2 h; Heating;
参考文献
Joucla, Marc; Mortier, Jacques
Bulletin de la Societe Chimique de France, 1988 , # 3 p. 579 - 583
141-32-2
丙烯酸丁酯
+
580-13-2
2-溴代萘
→
反应条件
124182-61-2
反应条件
sodium carbonate; silica supported Pd-NHC in N,N-dimethyl-formamide T=140°C; Mizoroki-Heck reaction; 20 h;
参考文献
Aksin, Oezge; Tuerkmen, Hayati; Artok, Levent; Cetinkaya, Bekir; Ni, Chaoying; Bueyuekguengoer, Orhan; Oezkal, Erhan
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 3027 - 3036
141-32-2
丙烯酸丁酯
+
93-11-8
2-萘磺酰氯
→
反应条件
124182-61-2
反应条件
potassium carbonate; benzyltrioctylammonium chloride; bis(benzonitrile)palladium(II) dichloride in m-xylene T=140°C; 4 h;
参考文献
Miura, Masahiro; Hashimoto, Hideo; Itoh, Kenji; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2207 - 2211
141-32-2
丙烯酸丁酯
+
2243-83-6
2-萘甲酰氯
→
反应条件
124182-61-2
反应条件
(benzyl)-tri-(butyl)-ammonium chloride; bis(benzonitrile)palladium(II) dichloride in o-xylene Mizoroki-Heck type arylation; 3 h; Heating;
参考文献
Sugihara, Toru; Satoh, Tetsuya; Miura, Masahiro
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8269 - 8271
91-20-3
萘
+
141-32-2
丙烯酸丁酯
→
反应条件
124182-61-2
反应条件
dirhodium tetraacetate; C2F3O2(1-)*Cu(2+); vanadium pentoxide; tri-cyclo-hexyl-phosphine in 1,2-dichloro-ethane T=140°C; 24 h; Schlenk techniqueMolecular sieveGloveboxInert atmosphere;
参考文献
Vora, Harit U.; Silvestri, Anthony P.; Engelin, Casper J.; Yu, Jin-Quan
Angewandte Chemie - International Edition, 2014 , vol. 53, # 10 p. 2683 - 2686
Angew. Chem., 2014 , vol. 126, # 10 p. 2721 - 2724,4
141-32-2
丙烯酸丁酯
+
2243-83-6
2-萘甲酰氯
→
反应条件
124182-61-2
反应条件
lithium chloride; [Rh(C2H4)2Cl]2 in xylene Mizoroki-Heck reaction; 5 h; Heating; Title compound not separated from byproducts;
参考文献
Sugihara, Toru; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1765 - 1772
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