(2-环己基-1,1-二氟乙基)-磷酸二乙酯合成路线 （共 4 条）
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene 12 h; Heating;
参考文献
Pignard, Sebastien; Lopin, Chrystel; Gouhier, Geraldine; Piettre, Serge R.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 31 - 37
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene 2 h; Heating;
参考文献
Martin; Dean; Wagman
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1839 - 1842
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.25 h / -78 °C 1.2: 71 percent / tetrahydrofuran; hexane / -78 - 20 °C 2.1: 82 percent / tri-n-butyltin hydride; azobis(isobutyronitrile) / toluene / 12 h / Heating View Scheme
参考文献
Martin; Dean; Wagman
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1839 - 1842
反应条件
2: 84 percent / tri-n-butyltin hydride, AIBN / toluene / 2 h / Heating View Scheme
参考文献
Martin; Dean; Wagman
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1839 - 1842
