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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
己酰氯
合成路线
（共 371 条）
109-87-5
甲缩醛
+
142-61-0
己酰氯
→
反应条件
106-70-7
己酸甲酯
+
107-30-2
氯甲基甲基醚
反应条件
T=55 - 60°C; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 59, # 21 p. 6499 - 6500
142-61-0
己酰氯
+
108-93-0
环己醇
→
反应条件
6243-10-3
己酸环己酯
反应条件
triethylamine 4 h; Heating;
参考文献
Pandey, Karuna Shanker; Mendki, Murlidhar Jaywantrao; Rao, Karumuru Mallikarjuna; Vaidyanathaswamy, Ramamoorthy
Bioscience, Biotechnology, and Biochemistry, 1995 , vol. 59, # 4 p. 725 - 727
142-61-0
己酰氯
→
反应条件
136-77-6
4-己基间苯二酚
反应条件
1: aluminum chloride / nitrobenzene / cooling 2: zinc amalgamate; conc. hydrochloric acid / ethanol; H2O / Heating View Scheme
参考文献
Mizobuchi, Shigeyuki; Sato, Yuko
Agricultural and Biological Chemistry, 1985 , vol. 49, # 5 p. 1327 - 1334
142-61-0
己酰氯
→
反应条件
133238-87-6
反应条件
1: triethylamine / dichloromethane / 1 h / 0 - 5 °C / |Inert atmosphere 2: AlCl3, aluminium chloride / nitrobenzene / 5 h / 140 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 2 h / 25 - 30 °C 4: bromine / dichloromethane / 1 h / 25 - 30 °C 5: AlCl3, aluminium chloride / dichloromethane / 15 - 20 °C 6: triethylamine / dichloromethane / 2 h / 25 - 30 °C 7: sodium tetrahydroborate / methanol / 0.5 h / 0 - 5 °C 8: hydrogenchloride / methanol; water / 5 h / 90 - 95 °C View Scheme
参考文献
Gopal, P. Raja; Chandrashekar; Saravanan; Bhaskar, B. Vijaya; Somaiah, P. Veera
Journal of Chemical Sciences, 2012 , vol. 124, # 5 p. 1077 - 1085
142-61-0
己酰氯
→
反应条件
141645-16-1
反应条件
1: triethylamine / dichloromethane / 1 h / 0 - 5 °C / |Inert atmosphere 2: AlCl3, aluminium chloride / nitrobenzene / 5 h / 140 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 2 h / 25 - 30 °C 4: bromine / dichloromethane / 1 h / 25 - 30 °C 5: AlCl3, aluminium chloride / dichloromethane / 15 - 20 °C 6: triethylamine / dichloromethane / 2 h / 25 - 30 °C 7: sodium tetrahydroborate / methanol / 0.5 h / 0 - 5 °C 8: hydrogenchloride / methanol; water / 5 h / 90 - 95 °C 9: AlCl3, aluminium chloride / dichloromethane / 5.08 h / 0 - 30 °C 10: AlCl3, aluminium chloride / chlorobenzene / 5.17 h / 20 - 80 °C View Scheme
参考文献
Gopal, P. Raja; Chandrashekar; Saravanan; Bhaskar, B. Vijaya; Somaiah, P. Veera
Journal of Chemical Sciences, 2012 , vol. 124, # 5 p. 1077 - 1085
142-61-0
己酰氯
→
反应条件
141627-42-1
反应条件
1: triethylamine / dichloromethane / 1 h / 0 - 5 °C / |Inert atmosphere 2: AlCl3, aluminium chloride / nitrobenzene / 5 h / 140 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 2 h / 25 - 30 °C 4: bromine / dichloromethane / 1 h / 25 - 30 °C 5: AlCl3, aluminium chloride / dichloromethane / 15 - 20 °C 6: triethylamine / dichloromethane / 2 h / 25 - 30 °C 7: sodium tetrahydroborate / methanol / 0.5 h / 0 - 5 °C 8: hydrogenchloride / methanol; water / 5 h / 90 - 95 °C 9: AlCl3, aluminium chloride / dichloromethane / 5.08 h / 0 - 30 °C View Scheme
参考文献
Gopal, P. Raja; Chandrashekar; Saravanan; Bhaskar, B. Vijaya; Somaiah, P. Veera
Journal of Chemical Sciences, 2012 , vol. 124, # 5 p. 1077 - 1085
142-61-0
己酰氯
→
反应条件
反应条件
暂无反应条件数据
参考文献
ECP ENICHEM POLIMERI S.r.l.
Patent: EP300800 A1, 1989 ;
142-61-0
己酰氯
→
反应条件
31450-61-0
反应条件
1: triethylamine / dichloromethane 2: water; lithium hydroxide hydrate / tetrahydrofuran View Scheme
参考文献
Wu, Yongwei; Singh, Ravi P.; Deng, Li
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12458 - 12461
142-61-0
己酰氯
+
74-89-5
→
反应条件
3418-05-1
反应条件
potassium carbonate in water; ethyl acetate
参考文献
Zyryanov, Grigory V.; Rudkevich, Dmitry M.
Organic Letters, 2003 , vol. 5, # 8 p. 1253 - 1256
142-61-0
己酰氯
+
31729-70-1
→
反应条件
32743-88-7
反应条件
in tetrahydrofuran T=25°C; Substitution;
参考文献
Matsubara, Seijiro; Yamamoto, Yuhei; Utimoto, Kiitiro
Synlett, 1999 , # 9 p. 1471 - 1473
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