Nef
Justus Liebigs Annalen der Chemie, 1904 , vol. 335, p. 323
Justus Liebigs Annalen der Chemie, 1907 , vol. 357, p. 215,300
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Evans
American Chemical Journal, 1906 , vol. 35, p. 124
Reppe et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 596, p. 65
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General Aniline and Film Corp.
Patent: US2273141 , 1938 ;
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I. G. Farbenind.
Patent: DE724759 , 1937 ;
DRP/DRBP Org.Chem.
in methanol org. acid suspending in Cu-compd. soln., stirring (12 h); filtration, washing (MeOH), drying (vac., 323 K); elem. anal.;
参考文献
Piper, J. D.; Fleiger, A. G.; Smith, C. C.; Kerstein, N. A.
Industrial and Engineering Chemistry, 1939 , vol. 31, p. 307 - 317
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Gmelin Handbook: Cu: MVol.B2, 44, page 715 - 717
Ramberg, L.
Z. phys. Ch., 1909 , vol. 69, p. 512 - 522
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Gmelin Handbook: Cu: MVol.B2, 26, page 676 - 679
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反应条件
in dichloromethane mixt. of copper(II) acetate and tin(II) 2-ethylhexanoate in CH2Cl2 is stirred at room temp. for 4 h; filtration, product is washed with CH2Cl2, solid dried in vacuo for several hours; elem. anal.;
参考文献
Lockhart, Thomas P.; Haitko, Deborah A.
Polyhedron, 1985 , vol. 4, p. 1745 - 1746
hydroxylammonium sulphate in ammonia warm soln.; great excess of NH4CH3COO; air excluded;; washed with acetic acid;;
参考文献
Pechard, E.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1903 , vol. 136, p. 504 - 506
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Gmelin Handbook: Cu: MVol.B2, 26, page 676 - 679