反应条件
n-butyllithium in hexane 1-chloroheptane (1 equiv.) and TMTH (1 equiv.) in hexane cooled to 0°C under Ar, n-BuLi (1 equiv., 2.40 M in hexane) added, stirred for 4 h, quenched with water; analyzed by GC;
参考文献
Organometallics, , vol. 6, p. 557 - 565