1-苯硫基-吡咯啉-2,5-二酮合成路线 （共 38 条）
反应条件
1: 98 percent / nBu3P / CH2Cl2 / 0 °C
2: 83 percent / Me3SiOOSiMe3 / benzene / 18 h / Heating
View Scheme
参考文献
Kocienski; Todd
Journal of the Chemical Society - Series Chemical Communications, 1982 , vol. No. 18, p. 1078 - 1079
反应条件
in triethylamine; benzene
参考文献
Eaton, Philip E.; Bunnelle, William H.; Engel, Peter
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2612 - 2626
反应条件
in triethylamine; benzene
参考文献
Eaton, Philip E.; Bunnelle, William H.; Engel, Peter
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2612 - 2626
反应条件
in benzene
20 h; Ambient temperature;
参考文献
Torii, Sigeru; Sayo, Noboru; Tanaka, Hideo
Chemistry Letters, 1980 , p. 695 - 698
反应条件
in toluene
Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
反应条件
palladium diacetate; trifluoroacetic acid
T=20°C; 0.75 h; Overall yield = 89 percent;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
sodium methylate
1.) CHCl3, -5-0 deg C, 20 min, 2.) CHCl3, -5-0 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Karpiesiuk, Wojciech; Sas, Wojciech
Journal of Chemical Research, Synopses, 1995 , # 3 p. 106 - 107
反应条件
p-toluenesulfonyl chloride in acetonitrile
T=20°C; Substitution; 7 h;
参考文献
Huang, Chih-Hao; Liao, Kang-Shyang; De, Surya Kanta; Tsai, Yeun-Min
Tetrahedron Letters, 2000 , vol. 41, # 20 p. 3911 - 3914
