[2-(氯甲基)苯基]甲醇合成路线 (共 13 条)
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Gharpure, Santosh J.; Reddy, S. Raja Bhushan; Sanyal, Udishnu
Synlett, 2007 , # 12 p. 1889 - 1892
反应条件
1: dimethylformamide / 6 h / Ambient temperature 2: potassium hydroxide / methanol; H2O / 2 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 360 - 362
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Journal of Organic Chemistry, , vol. 67, # 8 p. 2606 - 2618
反应条件
sodium periodate in dichloromethane T=40 - 50°C; Ionic liquid;
参考文献
Hullio, Ahmed Ali; Mastoi; Khan, Khalid
Asian Journal of Chemistry, 2011 , vol. 23, # 12 p. 5411 - 5418
反应条件
1: LiAlH4 / tetrahydrofuran 2: hydrochloric acid / H2O View Scheme
参考文献
Turro, Nicholas J.; Lei, Xue-Gong; Jockusch, Steffen; Li, Wei; Liu, Zhiqiang; Abrams, Lloyd; Ottaviani, M. Francesca
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2606 - 2618
反应条件
hydrogenchloride in water; toluene
T=70°C; 2 h;
参考文献
Showa Denko K.K.
Patent: US6372921 B1, 2002 ;
Location in patent: Example 24 ;
反应条件
sodium hydroxide in water
T=100°C; pH=7; 4 h;
参考文献
Showa Denko K.K.
Patent: US6372921 B1, 2002 ;
Location in patent: Example 17 ;
反应条件
hydrogenchloride in water
T=70°C; 1 h;
参考文献
Showa Denko K.K.
Patent: US6372921 B1, 2002 ;
Location in patent: Example 18 ;
反应条件
1: 94 percent / LiAlH4 / tetrahydrofuran
2: hydrochloric acid / H2O
View Scheme
参考文献
Turro, Nicholas J.; Lei, Xue-Gong; Jockusch, Steffen; Li, Wei; Liu, Zhiqiang; Abrams, Lloyd; Ottaviani, M. Francesca
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2606 - 2618
反应条件
Cellulosimicrobium cellulans EB-8-4
T=30°C; pH=7; 1 h; Microbiological reactionK-buffer containing glucoseEnzymatic reaction; chemoselective reaction;
参考文献
Dai, Shiyao; Wu, Jinchuan; Wang, Zunsheng; Chen, Yongzheng; Li, Zhi
Tetrahedron, 2010 , vol. 66, # 34 p. 6919 - 6923