[2-(氯甲基)苯基]甲醇合成路线 (共 13 条)
反应条件
Cellulosimicrobium cellulans EB-8-4
T=30°C; pH=7; 5 h; Microbiological reactionK-buffer containing glucoseEnzymatic reaction; chemoselective reaction;
参考文献
Dai, Shiyao; Wu, Jinchuan; Wang, Zunsheng; Chen, Yongzheng; Li, Zhi
Tetrahedron, 2010 , vol. 66, # 34 p. 6919 - 6923
反应条件
chloroformic acid ethyl ester; sodium hydrogencarbonate in benzene
1 h;
参考文献
Patil, Sharadbala D.; Mali, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 360 - 362
反应条件
1: 1) n-butyllithium / 1) ether, room temperature, 20 h, 2) room temperature, 2 h
2: ethyl chloroformate, sodium bicarbonate / benzene / 1 h
View Scheme
参考文献
Patil, Sharadbala D.; Mali, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 360 - 362