3-二氮杂-2-氧代丙酸乙酯合成路线 （共 20 条）
反应条件
in diethyl ether T=0°C; Inert atmosphere;
参考文献
Tetrahedron, , vol. 66, # 36 p. 7329 - 7332
反应条件
in tetrahydrofuran T=20°C; 12 h;
参考文献
Chemical Communications, , vol. 49, # 66 p. 7313 - 7315
反应条件
in tetrahydrofuran T=20°C; 3 h;
参考文献
Helvetica Chimica Acta, , vol. 88, # 5 p. 1010 - 1021
反应条件
in diethyl ether 1 h; Ambient temperature;
参考文献
Helvetica Chimica Acta, , vol. 80, # 5 p. 1375 - 1407
反应条件
1: NaOEt / diethyl ether 2: 2 percent / 2-azido-1-ethylpyridinium tetrafluoroborate, NaOAc, AcOH / H2O; ethanol / 1.17 h / Ambient temperature View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 105, # 5 p. 223 - 226
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 19, p. 1179,1188
参考文献
Bien,S.; Segal,Y.
Journal of Organic Chemistry, 1977 , vol. 42, p. 1685 - 1688
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
1: 76 percent / diethyl ether / 5 °C 2: 68 percent / H2O, AcOH / ethanol / 6 h / Ambient temperature View Scheme
参考文献
Ohsumi, Tadashi; Neunhoeffer, Hans
Tetrahedron, 1992 , vol. 48, # 25 p. 5227 - 5234
