triphenylphosphine; cyclopentadienyl sodium; hydrochloric acid in tetrahydrofuran; water Mo-complex in THF treated with PPh3 and CpNa (molar ratio 1:2:5) at room temp. for 20 min, treated with excess of aq. HCl at room temp. for 5 min;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 1 p. 30 - 31
tetrahydrofuran in tetrahydrofuran soln. Kptc in THF added slowly to mixt. Mo2(OAc)4 in THF and stirred for 1 h; KOAc filtered, volume soln. reduced, hexane added and refrigerated for several days;
参考文献
Bereman, Robert D.; Baird, Donald M.; Moreland, Charles G.
Polyhedron, 1983 , vol. 2, p. 59 - 62
