1: sodium tetraphenyl borate With Amberlite(R)IRA-900 resin in water
2: 3-(bromo)-quinoline With tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl-formamide
T=80°C; Suzuki-Miyaura coupling reaction; 4 h; Further stages.;
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; mole ratio NaBPh4 : CuI = 1 : 1; irradn. (254 nm) for 1 h gave deposition of Cu; deposit sepd., washed with acetone and water, and dried in vac. to give pure Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; mole ratio NaBPh4 : CuBr2 = 2 : 1; irradn. (254 nm) for 8 h gave deposition of Cu; deposit sepd., washed with acetone and water, and dried in vac. to give pure Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; mole ratio NaBPh4 : Cu(acac)2 = 2 : 1; irradn. (254 nm) for 18 h gave deposition of Cu; deposit sepd., washed with acetone and water, and dried in vac. to give pure Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; mole ratios NaBPh4 : NiBr2 : CuBr2 = 8 : 3 : 1; irradn. (254 nm) for 10 h gave deposition of Ni and Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; mole ratios NaBPh4 : SnCl2 : CuBr2 = 4 : 1 : 1; irradn. (254 nm) for 14 h gave deposition of Co and Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; mole ratios NaBPh4 : CoCl2 : CuBr2 = 4 : 1 : 1; irradn. (254 nm) for 10 h gave deposition of Co and Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
in ethylene glycol dimethyl ether
Irradiation (UV/VIS); under Ar; ratios B(3+) : Ni(2+) : Cu(2+) = 4 : 1 : 1; irradn. (254 nm) for 18 h gave deposition of Ni and Cu;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
