1-乙基-3-甲基咪唑四氟硼酸盐合成路线 (共 15 条)
反应条件
potassium tetrafluoroborate T=70°C; 4 h;
参考文献
Journal of Fluorine Chemistry, , vol. 129, # 2 p. 108 - 111
反应条件
tetrafluoroboric acid; silver(l) oxide in water T=20°C; Substitution; 2 h;
参考文献
Journal of the Chemical Society - Dalton Transactions, , # 13 p. 2133 - 2139
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in acetonitrile T=20°C; Mitsunobu reaction;
参考文献
Tetrahedron Letters, , vol. 49, # 22 p. 3663 - 3665
反应条件
tetrafluoroboric acid in water T=20°C;
参考文献
WO2006/7912 A1, ;
Page/Page column 21-22 ;
反应条件
1: T=50°C; 2: With sodium tetrafluoroborate in acetone T=20°C; 48 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 25 p. 8395 - 8401
反应条件
in diethyl ether 20 h;
参考文献
Journal of Fluorine Chemistry, , vol. 127, # 9 p. 1261 - 1264
参考文献
Chemical Physics Letters, , vol. 461, # 4-6 p. 229 - 234
反应条件
1: hydrogen fluoride; boron trifluoride in ethanol T=5°C; 2: 1-ethyl-3-methyl imidazolium 2-hydroxyisobutyric acid salt in ethanol 1 h; Product distribution / selectivity;
参考文献
WO2006/90657 A1, ;
Page/Page column 19 ;
反应条件
in methanol T=0°C; Product distribution / selectivity;
参考文献
WO2006/90657 A1, ;
Page/Page column 17-18 ;
反应条件
in diethyl ether 2 h; cooling;
参考文献
Chemistry Letters, , vol. 37, # 7 p. 682 - 683