3,5-二-叔-丁基-4-羟基苄基乙酸酯合成路线 （共 50 条）
反应条件
perchloric acid; water in acetone 28 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2765 - 2770
反应条件
perchloric acid in acetone 1) heating, 2) 24 h, 20 deg C;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2765 - 2770
反应条件
in N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
Bukharov; Nugumanova; Mukmeneva
Russian Journal of General Chemistry, 2003 , vol. 73, # 3 p. 408 - 412
反应条件
cobalt(III) acetate in acetic acid T=50°C; 15 h;
参考文献
Hirano, Masao; Ishii, Tadamichi; Morimoto, Takashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1434 - 1436
反应条件
hydrogenchloride in ethylene glycol dimethyl ether; hexane
参考文献
Grinter; Trevor John; Hayler; John David; Negus; Alan; Harris; Michael Anthony
Patent: US6048995 A1, 2000 ;
反应条件
sulfuric acid in acetic acid T=60°C; 6 h;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 9 ;
反应条件
sulfuric acid in acetic acid T=60°C; 3 h;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 9 ;
反应条件
sulfuric acid in acetic acid T=20 - 60°C; 27 h; Inert atmosphere;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 9-10 ;
反应条件
potassium acetate in hexane; acetone
参考文献
Grinter; Trevor John; Hayler; John David; Negus; Alan; Harris; Michael Anthony
Patent: US6048995 A1, 2000 ;
反应条件
diethylamine
11 h; Reflux;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 8-9 ;
