3,5-二-叔-丁基-4-羟基苄基乙酸酯合成路线 （共 50 条）
反应条件
diethylamine
T=20 - 110°C; 6 h; Reflux;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 10-11 ;
反应条件
water in acetone
1) 1h, reflux, 2) after addition of water 1h, reflux;
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
bromine; acetic acid
参考文献
Coppinger; Campbell
Journal of the American Chemical Society, 1953 , vol. 75, p. 734
反应条件
toluene-4-sulfonic acid; acetic acid
参考文献
Coppinger
Journal of the American Chemical Society, 1957 , vol. 79, p. 2758
参考文献
Coppinger; Campbell
Journal of the American Chemical Society, 1953 , vol. 75, p. 734
反应条件
cobalt(III) acetate in acetic acid
T=50°C; 15 h;
参考文献
Hirano, Masao; Ishii, Tadamichi; Morimoto, Takashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1434 - 1436
反应条件
1: platinum/charcoal; isooctane / Hydrogenation
2: acetic acid; toluene-4-sulfonic acid
View Scheme
参考文献
Coppinger
Journal of the American Chemical Society, 1957 , vol. 79, p. 2758
反应条件
1: LiAlH4; diethyl ether
2: acetyl chloride
View Scheme
参考文献
Coppinger; Campbell
Journal of the American Chemical Society, 1953 , vol. 75, p. 734
反应条件
1: With 5 palladium on charcoal; potassium acetate in water
T=100°C; 0.333333 h;
2: With oxygen in water
8 h;
参考文献
Barton, Benita; Logie, Catherine G.; Schoonees, Barbara M.; Zeelie, Bernard
Organic Process Research and Development, 2005 , vol. 9, # 1 p. 62 - 69
反应条件
bromine; acetic acid
参考文献
Coppinger; Campbell
Journal of the American Chemical Society, 1953 , vol. 75, p. 734
