1: salicylic acid With potassium carbonate in acetone T=20°C; 0.166667 h; 2: benzyl bromide in acetone 18 h; RefluxInert atmosphere;
参考文献
Johnson, Myron M.; Naidoo, Jeremy M.; Fernandes, Manuel A.; Mmutlane, Edwin M.; Van Otterlo, Willem A. L.; De Koning, Charles B.
Journal of Organic Chemistry, 2010 , vol. 75, # 24 p. 8701 - 8704
potassium carbonate in N,N-dimethyl-formamide benzylation; 2 h; Heating;
参考文献
Silva, Artur M. S.; Almeida, Lucia M. P. M.; Cavaleiro, Jose A. S.; Foces-Foces, Concepcion; Llamas-Saiz, Antonio L.; Fontenas, Christophe; Jagerovic, Nadine; Elguero, Jose
Tetrahedron, 1997 , vol. 53, # 34 p. 11645 - 11658
sodium hydroxide in methanol; water T=60 - 70°C; Hydrolysis; 3 h;
参考文献
Silva, Artur M. S.; Almeida, Lucia M. P. M.; Cavaleiro, Jose A. S.; Foces-Foces, Concepcion; Llamas-Saiz, Antonio L.; Fontenas, Christophe; Jagerovic, Nadine; Elguero, Jose
Tetrahedron, 1997 , vol. 53, # 34 p. 11645 - 11658
1: NaOH / aq. ethanol / 15 h / Heating
2: oxalyl chloride, DMF / CH2Cl2 / 3 h / 0 °C
View Scheme
参考文献
Ye, Tao; Garcia, Concepcion Fernandez; McKervey, M. Anthony
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1373 - 1380
