5-(3-吡啶基)-1H-吲哚合成路线 （共 3 条）
反应条件
1: With palladium diacetate; xantphos in N-dodecane; butan-1-ol T=25°C; Suzuki-Miyaura Coupling; 0.25 h; Inert atmosphereGlovebox; 2: With cesium hydroxide monohydrate in N-dodecane; water; butan-1-ol T=25°C; Suzuki-Miyaura Coupling; Inert atmosphereGlovebox;
参考文献
Yang, Junfeng; Liu, Sijia; Zheng, Jian-Feng; Zhou, Jianrong
European Journal of Organic Chemistry, 2012 , # 31 p. 6248 - 6259,12
Title/Abstract Full Text Show Details
Yang, Junfeng; Liu, Sijia; Zheng, Jian-Feng; Zhou, Jianrong
European Journal of Organic Chemistry, 2012 , # 31 p. 6248 - 6259
反应条件
1: 3-bromo-pyridine With AlCl3, aluminium chloride; magnesium; lithium chloride in tetrahydrofuran T=25°C; 4 h; Schlenk techniqueInert atmosphere; 2: 5-Bromo-1H-indole With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran T=50°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Bernhardt, Sebastian; Shen, Zhi-Liang; Knochel, Paul
Chemistry - A European Journal, 2013 , vol. 19, # 3 p. 828 - 833
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate in ethylene glycol dimethyl ether 4 h; Heating;
参考文献
Yang, Youhua; Martin, Arnold R.
Heterocycles, 1992 , vol. 34, # 7 p. 1395 - 1398
