N,N-二甲基-苯磺酰胺合成路线 （共 44 条）
反应条件
tin(IV) chloride Heating;
参考文献
Mizhiritskii, M. D.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 7 p. 1547 - 1558,1373 - 1382
参考文献
Naddaka, V. I.; Avanesyan, K. V.; Cherkinskaya, M. L.; Minkin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 4 p. 801 - 802
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 4 p. 885 - 886
反应条件
1: Et3N / CH2Cl2 / -70 °C 2: CH2Cl2 / 25 °C View Scheme
参考文献
Banks, Malcolm R.; Hudson, Robert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 151 - 156
反应条件
in diethyl ether T=-10°C;
参考文献
Ruosteuso, P.; Haekkinen, A.-M.; Mattila, T.
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 189 - 193
反应条件
1.1: N-bromosuccinmide / N,N-dimethyl-formamide / 0.5 h / 20 °C 2.1: trifluorormethanesulfonic acid / toluene / 1 h / 0 °C / |Inert atmosphere 2.2: 24 h / 0 - 20 °C / |Inert atmosphere 3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / |Inert atmosphere 3.2: 1.5 h / -78 - 0 °C / |Inert atmosphere 3.3: 1 h / -78 °C / |Inert atmosphere View Scheme
参考文献
Fukuda, Tsutomu; Iwao, Masatomo
Heterocycles, 2012 , vol. 86, # 2 p. 1261 - 1273
反应条件
1.1: trifluorormethanesulfonic acid / toluene / 1 h / 0 °C / |Inert atmosphere 1.2: 24 h / 0 - 20 °C / |Inert atmosphere 2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / |Inert atmosphere 2.2: 1.5 h / -78 - 0 °C / |Inert atmosphere 2.3: 1 h / -78 °C / |Inert atmosphere View Scheme
参考文献
Fukuda, Tsutomu; Iwao, Masatomo
Heterocycles, 2012 , vol. 86, # 2 p. 1261 - 1273
参考文献
Naddaka, V. I.; Avanesyan, K. V.; Cherkinskaya, M. L.; Minkin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 4 p. 801 - 802
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 4 p. 885 - 886
反应条件
sodium hydroxide 1 h; Yield given. Yields of byproduct given;
参考文献
Goodrow, Marvin, H.; Musker, W. Kenneth
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3332 - 3333
参考文献
Hansch; Silipo
Journal of Medicinal Chemistry, 1974 , vol. 17, # 7 p. 661 - 667
参考文献
Jones; Whalen
Journal of the American Chemical Society, 1925 , vol. 47, p. 1347
