双(2-氰乙基)丙二酸二乙酯合成路线 （共 22 条）
参考文献
US2396626 , ;
DE732743 , ;
DRP/DRBP Org.Chem.
参考文献
Justus Liebigs Annalen der Chemie, , vol. 563, p. 35
反应条件
1: 60 percent / hydrogen / Raney-Ni / ethanol 2: 1.) sodium hydride / 1.) DMSO, 65-70 deg C View Scheme
参考文献
Bell; Choi; Hiel
Tetrahedron Letters, 1993 , vol. 34, # 6 p. 971 - 974
反应条件
hydrogenchloride; water
Hydrolysis; Decarboxylation; 72 h; Heating;
参考文献
Suissa, M. Rachel; Romming, Christian; Dale, Johannes
Chemistry - A European Journal, 1999 , vol. 5, # 10 p. 3055 - 3065
反应条件
hydrogen; nickel in ethanol
参考文献
Bell; Choi; Hiel
Tetrahedron Letters, 1993 , vol. 34, # 6 p. 971 - 974
反应条件
1: concentrated aqueous hydrochloric acid
2: 1,2-dichloro-ethane; sulfuric acid / unter Entfernen des gebildeten Wassers
View Scheme
参考文献
Koehler et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5779,5782
反应条件
1: concentrated aqueous hydrochloric acid
2: PbO
View Scheme
参考文献
Mariella et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 1702,1707
参考文献
Clemo; Tenniswood
Journal of the Chemical Society, 1931 , p. 2551
反应条件
1: 87 percent / HCl; H2O / 72 h / Heating
2: 83 percent / H2SO4 / 96 h / Heating
View Scheme
参考文献
Murthi, G. S. S.; Mazumder, Alok
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. <B> 20, # 4 p. 339 - 340
反应条件
1: concentrated aqueous hydrochloric acid
2: PbO
3: benzyl-trimethyl-ammonium hydroxide
View Scheme
参考文献
Mariella et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 1702,1707
