(S)-(-)-1-苯基乙醇合成路线 （共 393 条）
反应条件
oxonium; methyllithium 1.) ether; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 22, # 44 p. 4417 - 4420
反应条件
Pseudomonas cepacia lipase in diethyl ether T=77°C; 3 h; Irradiationwithout MW irradiation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 22 p. 7746 - 7749
反应条件
Candida antarctica lipase in diethyl ether T=90°C; 0.25 h; Irradiationwithout MW irradiation; other temperature, reaction time; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 22 p. 7746 - 7749
反应条件
Pseudomonas cepacia lipase in diethyl ether T=85°C; 0.25 h; Irradiationwithout MW irradiation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 22 p. 7746 - 7749
反应条件
water; acetic acid; sodium nitrite 1.) RT, 18 h, 2.) 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 13 p. 2193 - 2198
反应条件
(-)-2,3-O-isopropylidene-1,1,4,4-tetraphenyl-L-threitol; tantalum pentachloride in dichloromethane 40 h; Ambient temperatureenantioselective acylation of various secondary alcohols with other chiral reagent; kinetic resolution; Product distribution;
参考文献
Tetrahedron Letters, , vol. 39, # 20 p. 3263 - 3266
反应条件
methylmagnesium bromide in dichloromethane T=0°C; Acylation; 6 h; Product distribution; Further Variations:SolventsTemperaturesReagents;
参考文献
Journal of Organic Chemistry, , vol. 64, # 26 p. 9365 - 9373
反应条件
1: 1.) ZnCl2, 2.) i-Bu2AlH / 1.) THF, r.t., 0.5 h, 2.) toluene, -100 deg C, 0.6 h 2: Raney-Ni View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 211 - 213
反应条件
lipase LipK107 from Proteus sp. E130L and K131I mutant; water in 2,2,4-trimethylpentane T=20°C; 24 h; Resolution of racemateEnzymatic reaction; Kinetics; Reagent/catalyst; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 68, # 3-4 p. 286 - 291
反应条件
water T=30°C; 168 h; asymmetric hydrolysis and resolution by Pseudomonas cepacia; Product distribution;
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 58, # 7 p. 1330 - 1331
