1.1: n-BuLI / tetrahydrofuran / 0.5 h / 0 °C
1.2: tetrahydrofuran / 4 h / 20 °C
2.1: Bu4NF / tetrahydrofuran / 8 h / 26 °C
View Scheme
参考文献
Madhushaw, Reniguntala J.; Lin, Ming-Yuan; Abu Sohel, Shariar Md.; Liu, Rai-Shung
Journal of the American Chemical Society, 2004 , vol. 126, # 22 p. 6895 - 6899
1: triphenylbenzyl-phosphonium bromide With n-butyllithium in tetrahydrofuran
T=0°C; 0.5 h;
2: 2-(2-trimethylsilyleth-1-yn-1-yl)benzaldehyde in tetrahydrofuran
T=20°C; 4 h;
参考文献
Madhushaw, Reniguntala J.; Lin, Ming-Yuan; Abu Sohel, Shariar Md.; Liu, Rai-Shung
Journal of the American Chemical Society, 2004 , vol. 126, # 22 p. 6895 - 6899
Karatsu, Takashi; Kitamura, Akihide; Arai, Tatsuo; Sakuragi, Hirochika; Tokumaru, Katsumi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 6 p. 1674 - 1679
