1,1'-(亚甲二氧基)二环己烷合成路线 (共 38 条)
反应条件
Montmorillonite K 10 6 h; Heating;
参考文献
Deshmukh; Gumaste; Bhawal
Synthetic Communications, 1995 , vol. 25, # 24 p. 3939 - 3944
反应条件
toluene-4-sulfonic acid T=60°C;
参考文献
Danikiewicz; Szmigielski
Synthetic Communications, 2001 , vol. 31, # 19 p. 3047 - 3054
反应条件
sodium hydroxide; 4 A molecular sieve; silver carbonate 1.) CH2Cl2, room temp. 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Chaudhuri, Subrata Kumar; Pramanik, Amit; Roy, Rimi; Khan, Sagar; Ghatak, Avishek; Bhar, Sanjay
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1773 - 1780
反应条件
potassium hydroxide; methyl-tridecylammonium chloride Heating;
参考文献
Dehmlow,E.V.; Schmidt,J.
Tetrahedron Letters, 1976 , p. 95 - 96
参考文献
Setkina et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 750,753; engl. Ausg. S. 667, 670
参考文献
Setkina et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 750,753; engl. Ausg. S. 667, 670
参考文献
Olsen
Zeitschrift fuer Naturforschung, 1946 , vol. 1, p. 680
反应条件
di-tert-butyl peroxide T=130°C; other temperatures.; Product distributionRate constantMechanism;
参考文献
Kalashnikov, S. M.; Imashev, U. B.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 12 p. 2798 - 2802,2267 - 2271
反应条件
chloroform; di-tert-butyl peroxide T=130°C; 1.5 h; glass ampul; Product distributionMechanism;
参考文献
Rol'nik, L.Z.,; Kalashnikov, S.M.; Pastushenko, E.V.; Zlotskii, S.S.; Imashev, U.B.,; Rakhmankulov, D.L.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 457 - 459
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 3 p. 539 - 540