1,1'-(1,3-丙烷二基)二萘合成路线 （共 6 条）
反应条件
sodium amide in benzene T=90°C; 3 h;
参考文献
Blank, Norman E.; Haenel, Matthias W.
Chemische Berichte, 1981 , vol. 114, # 4 p. 1531 - 1538
反应条件
1: H2 / Pd-C 2: N2H4*H2O, NaOH View Scheme
参考文献
Chandross,E.A.; Dempster,C.J.
Journal of the American Chemical Society, 1970 , vol. 92, # 12 p. 3586 - 3593
反应条件
sodium hydroxide; hydrazine hydrate in water; diethylene glycol 1.) 120 deg C, 2 h, 2.) 200 deg C, 6 h;
参考文献
Gruetzmacher, Hans-Friedrich; Nolte, Gerald
Chemische Berichte, 1994 , vol. 127, # 6 p. 1157 - 1162
反应条件
sodium hydroxide; hydrazine hydrate
参考文献
Chandross,E.A.; Dempster,C.J.
Journal of the American Chemical Society, 1970 , vol. 92, # 12 p. 3586 - 3593
反应条件
1: 1.) i-PrMgBr, 2.) 7N HCl / 1.) Et2O, r.t., 2 h, 2.) glacial CH3COOH, reflux, 5 h 2: 64 percent / 80percent N2H4, NaOH / bis-(2-hydroxy-ethyl) ether; H2O / 1.) 120 deg C, 2 h, 2.) 200 deg C, 6 h View Scheme
参考文献
Gruetzmacher, Hans-Friedrich; Nolte, Gerald
Chemische Berichte, 1994 , vol. 127, # 6 p. 1157 - 1162
反应条件
1: H2SO4 2: 1.) i-PrMgBr, 2.) 7N HCl / 1.) Et2O, r.t., 2 h, 2.) glacial CH3COOH, reflux, 5 h 3: 64 percent / 80percent N2H4, NaOH / bis-(2-hydroxy-ethyl) ether; H2O / 1.) 120 deg C, 2 h, 2.) 200 deg C, 6 h View Scheme
参考文献
Gruetzmacher, Hans-Friedrich; Nolte, Gerald
Chemische Berichte, 1994 , vol. 127, # 6 p. 1157 - 1162
