反应条件
in neat (no solvent) inert atmosphere; slow addn. of dichlorostibine to excess of Bu3SnH (room temp.) with continuous fractional distn. of product (vac., condensingat -196°C); Z-isomer present in traces (NMR);
参考文献
Legoupy, S.; Lassalle, L.; Guillemin, J.-C.; Metail, V.; Senio, A.; Pfister-Guillouzo, G.
Inorganic Chemistry, 1995 , vol. 34, p. 1466 - 1471
