Delmond, B.; Pommier, J. C.; Valade, J.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1972 , vol. 275, p. 1037 - 1040
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Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.7, page 69 - 97
butyl bromide in neat (no solvent, gas phase) cocondn. on surface cooled with liq. nitrogen (reaction vessel (vac. ca. 1E-5 mm) in Dewar vessel, tin atomization with STP-30 stabilized powersupply, proportion of Sn:alkyl halide vapor 1:10 to 1:1000),reaction vessel removal from Dewar vessel; reaction mixt. dissoln. (ethanol), soln. filtration, alcohol transcondn. (vac.), powder exposing to vac. for several d; elem. anal.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 52, p. 2283 - 2287
Zhurnal Obshchei Khimii, , vol. 52, p. 2583 - 2588
PhCH2Pd(PPh3)2Cl in toluene T=110°C; 16 h; other tri(n-butyl)stannanes, other catalysts, other solvents, various reaction temperature and time; Product distribution;
