Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.4.5, page 106 - 108
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Carlisle Chemical Works, Inc.
Patent: NL6513659 , 1966 ;
C.A., 1966 , vol. 65, p. 7218
in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, , vol. 22, # 3 p. 246 - 247