二(三甲基甲硅烷基)乙炔合成路线 （共 218 条）
反应条件
in deuterated toluene (N2); a soln. of Ti-complex and diphenylacetylene heated to 85°Cfor 6 h; monitored by (1)H NMR;
参考文献
Tebbe,F.N.; Harlow,R.L.
Journal of the American Chemical Society, 1980 , vol. 102, p. 6149
反应条件
in benzene 5 h; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 2324
反应条件
hydroxytriphenylsilane; hexacarbonyl molybdenum in octane 0.25 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 42, # 22 p. 3701 - 3703
反应条件
18-crown-6 ether; cesium fluoride in benzene (Ar); room temp.;
参考文献
Journal of Organometallic Chemistry, , vol. 634, # 1 p. 69 - 73
反应条件
in benzene all manipulations under dry Ar; heating benzene soln. of 2,3-benzo-7,7-dimethyl-1,4,5,6-tetraphenyl-7-germanorborna-2,5-diene and bis(trimethylsilyl)thioketene (70°C, 3 h); preparative GLC (10percent SF-96 on Celite 545);
参考文献
Organometallics, , vol. 8, p. 1467 - 1472
反应条件
in various solvent(s) T=100°C;
参考文献
Chemische Berichte, , vol. 127, # 5 p. 813 - 820
反应条件
T=650°C; P=0.001 Torr; Further byproducts given;
参考文献
Chemistry Letters, , # 8 p. 1441 - 1444
反应条件
lithium in tetrahydrofuran
参考文献
Journal of Organometallic Chemistry, , vol. 18, p. 55 - 67
反应条件
in benzene 2 h; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 2324
反应条件
in toluene (N2); at room temp.;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 6149
