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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
14635-91-7
合成路线
（共 30 条）
625-95-6
3-碘甲苯
+
536-74-3
苯乙炔
→
反应条件
14635-91-7
反应条件
copper(l) iodide; iron; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=110°C; Sonogashira coupling; 1 h; Inert atmosphere;
参考文献
Tran, Ngoc Thang; Cho, Chan Sik; Sohn, Ho-Sang; Shim, Sang Chul
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 3 p. 1080 - 1082
591-17-3
3-溴甲基苯
+
536-74-3
苯乙炔
→
反应条件
14635-91-7
反应条件
pyrrolidine; bis(η3-allyl-μ-chloropalladium(II)); Br(1-)*C15H18N2O2P(1+); 1-n-butyl-3-methylimidazolium tetrafluoroborate T=125°C; Heck reaction; 40 h; Inert atmosphere;
参考文献
Saleh, Samer; Fayad, Elie; Azouri, Michele; Hierso, Jean-Cyrille; Andrieu, Jacques; Picquet, Michel
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 10 p. 1621 - 1628
591-50-4
碘苯
+
766-82-5
3-甲基苯乙炔
→
反应条件
14635-91-7
反应条件
bis-triphenylphosphine-palladium(II) chloride; (+/-)-Butanamine in water T=25°C; Sonogashira coupling; 1.5 h; Inert atmosphere;
参考文献
Komaromi, Anna; Tolnai, Gergely Laszlo; Novak, Zoltan
Tetrahedron Letters, 2008 , vol. 49, # 51 p. 7294 - 7298
591-50-4
碘苯
+
625-95-6
3-碘甲苯
+
115-19-5
2-甲基-3-丁炔-2-醇
→
反应条件
14635-91-7
反应条件
1: 3-methyliodobenzene; 2-methyl-but-3-yn-2-ol With copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; Sonogashira coupling; 1 h; 2: iodobenzene With sodium hydride T=110°C; Sonogashira coupling;
参考文献
Novak, Zoltan; Nemes, Peter; Kotschy, Andras
Organic Letters, 2004 , vol. 6, # 26 p. 4917 - 4920
108-41-8
3-氯甲苯
+
536-74-3
苯乙炔
→
反应条件
14635-91-7
反应条件
caesium carbonate; PdCl(C6H3-2,6-(OPiPr2)); zinc(II) chloride in 1,4-dioxane T=160°C; 24 h;
参考文献
Eberhard, Michael R.; Wang, Zhaohui; Jensen, Craig M.
Chemical Communications, 2002 , # 8 p. 818 - 819
17933-03-8
3-甲基苯硼酸
+
637-44-5
苯丙炔酸
→
反应条件
14635-91-7
反应条件
C16H14N2O4Pd; silver(l) oxide in dichloromethane T=20°C; 12 h;
参考文献
Heo, Yumi; Kang, Yi Young; Palani, Thiruvengadam; Lee, Junseong; Lee, Sunwoo
Inorganic Chemistry Communications, 2012 , vol. 23, p. 1 - 5
766-82-5
3-甲基苯乙炔
+
98-80-6
苯硼酸
→
反应条件
14635-91-7
反应条件
2,6-dimethylpyridine; oxygen; copper(I) bromide in methanol T=45°C; Sonogashira coupling; P=760.051 Torr; 16 h;
参考文献
Yasukawa, Tomohiro; Miyamura, Hiroyuki; Kobayashi, Sh
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 18 p. 6208 - 6210
766-82-5
3-甲基苯乙炔
+
108-90-7
氯苯
→
反应条件
14635-91-7
反应条件
palladium 10 on activated carbon; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl acetamide T=110°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Komaromi, Anna; Novak, Zoltan
Chemical Communications, 2008 , # 40 p. 4968 - 4970
625-95-6
3-碘甲苯
+
637-44-5
苯丙炔酸
→
反应条件
14635-91-7
反应条件
1: 3-phenyl-2-propynoic acid With silver(l) oxide in N,N-dimethyl-formamide T=20°C; 0.0833333 h; Inert atmosphere; 2: 3-methyliodobenzene With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine; lithium iodide in N,N-dimethyl-formamide T=100°C; Sonogashira coupling; 0.5 h; Inert atmosphere;
参考文献
Kim, Hyunseok; Lee, Phil Ho
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 17 p. 2827 - 2832
17933-03-8
3-甲基苯硼酸
+
536-74-3
苯乙炔
→
反应条件
14635-91-7
反应条件
potassium acetate; silver(l) oxide in dichloromethane T=20°C; 24 h;
参考文献
Yang, Fan; Wu, Yangjie
European Journal of Organic Chemistry, 2007 , # 21 p. 3476 - 3479
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