2,5-双(氯甲基)-4-(2-乙基己氧基)苯甲醚合成路线 （共 6 条）
反应条件
hydrogenchloride in 1,4-dioxane a) RT, 3 d, b.) reflux, 3.5 h;
参考文献
Burn, Paul L.; Kraft, Arno; Baigent, Derek R.; Bradley, Donal D. C.; Brown, Adam R.; Friend, Richard H.; Gymer, Richard W.; Holmes, Andrew B.; Jackson, Roger W.
Journal of the American Chemical Society, 1993 , vol. 115, # 22 p. 10117 - 10124
反应条件
1: KOH / methanol / Heating 2: 54 percent / HCl; H2SO4 / dioxane / Heating View Scheme
参考文献
Molecular Crystals and Liquid Crystals, , vol. 459, # 1 p. 141/[421]-153/[433]
反应条件
1: 1.) NaOMe / 1.) MeOH, reflux, 30 min, 2.) MeOH, reflux, 18 h 2: 79 percent / aq. HCl, HCl(gas) / dioxane / a) RT, 3 d, b.) reflux, 3.5 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 22 p. 10117 - 10124
反应条件
water; calcium carbonate in 1,4-dioxane
参考文献
Cho, Nam Sung; Hwang, Do-Hopn; Jung, Byung-Jun; Lim, Eunhee; Lee, Jaemin; Shim, Hong-Ku
Macromolecules, 2004 , vol. 37, # 14 p. 5265 - 5273
反应条件
in N,N-dimethyl-formamide T=45°C; 72 h;
参考文献
Cho, Nam Sung; Hwang, Do-Hopn; Jung, Byung-Jun; Lim, Eunhee; Lee, Jaemin; Shim, Hong-Ku
Macromolecules, 2004 , vol. 37, # 14 p. 5265 - 5273
反应条件
2-Nitropropane; sodium ethanolate in ethanol; dimethyl sulfoxide
参考文献
Cho, Nam Sung; Hwang, Do-Hopn; Jung, Byung-Jun; Lim, Eunhee; Lee, Jaemin; Shim, Hong-Ku
Macromolecules, 2004 , vol. 37, # 14 p. 5265 - 5273
