反应条件
Li in propan-1-ol Li was dissolved in PrOH at room temp. under N2; phthalonitrile was added; stirred at 75°C for 12 min; CuCl2 was added; reacted for 30 min; evapd. (vac.); dissolved in CH2Cl2; filtered; filtrate chromd. (alumina,CH2Cl2); concd. (vac., below 40°C); hexane added; elem. anal.;
参考文献
Fukuda, Takamitsu; Kikukawa, Yuu; Tsuruya, Ryota; Fuyuhiro, Akira; Ishikawa, Naoto; Kobayashi, Nagao
Inorganic Chemistry, 2011 , vol. 50, # 22 p. 11832 - 11837
