反应条件
HCl; NaOH or Na2CO3 in water HCl addn to Rh-salt, soln. evapn., water addn., mixt. evapn. to dryness,residue dissoln. (H2O), org. ligand addn., soln. boiling (ca. 2 h, cons t. vol.), pH 6.0-6.5 (NaOH or Na2CO3), boiling, cooling, Rh filtration off, filtrate evapn. to small vol.; ppt. filtration after cooling, filtrate and wash water evapn. to small vol., ppt. sepn., procedure repeating several times (filtrate pH adjusting to 6.0-6.5, at least to 9.0-10.0), ppts. collection, washing (water, ethanol), vac. drying; elem. anal.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 26, p. 82 - 84
Zhurnal Neorganicheskoi Khimii, , vol. 26, p. 156 - 159