反应条件
1: hydrogen chloride 2: K2CO3 / CH2Cl2; triethylamine / 48 h / Ambient temperature 3: 98 percent / Et4NOTs / 5.8 F/mol of electricity 4: 73 percent / acetic acid / 4 h / 100 °C 5: 1) Me4NCl/e, methanolic HCl, 2) NaOH / 1) CH3OH, 2) 33percent ethanol/water, room temperature View Scheme
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Tsubata, Kenji; Uchida, Kenshi; Kanazawa, Takenobu; Tsuda, Kunio
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3711 - 3716