1-(3,4-二氯苯基)乙醇合成路线 (共 10 条)
反应条件
anhydrous lithium nitrate in methanol T=30°C; 0.166667 h;
参考文献
Fernandes, Jane Luiza Nogueira; De Souza, Marcos Costa; Brenelli, Eugenia Cristina Souza; Brenelli, Jose Afranio
Synthesis, 2009 , # 23 art. no. M03909SS, p. 4058 - 4062
参考文献
Organic Syntheses, , vol. Coll. Vol. III, p. 200
Journal of the American Chemical Society, , vol. 68, p. 861,863
Industrial and Engineering Chemistry, , vol. 39, p. 1486,1487
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1295,1297
Journal of the American Chemical Society, , vol. 68, p. 1105,1107
反应条件
1: AlCl3 2: isopropyl alcohol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1105,1107
反应条件
Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 78, p. 5612
反应条件
Hydrogenation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 22, p. 93
反应条件
toluene-4-sulfonic acid in benzene 4 h;
参考文献
Efange, Simon M. N.; Kamath, Ashok P.; Khare, Anil B.; Kung, Mei-Ping; Mach, Robert H.; Parsons, Stanley M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 24 p. 3905 - 3914
反应条件
chromium(VI) oxide; acetic acid
参考文献
Zdansky
Arkiv foer Kemi, 1955 , vol. 7, p. 577,578
反应条件
1: 1-(3,4-dichlorophenyl)ethanol With sodium hydride in tetrahydrofuran
T=20°C; 0.5 h;
2: trichloroacetonitrile in tetrahydrofuran
T=20°C; 2 h;
参考文献
Yasuhara, Akito; Sakagami, Kazunari; Yoshikawa, Ryoko; Chaki, Shigeyuki; Nakamura, Masato; Nakazato, Atsuro
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 10 p. 3405 - 3420
反应条件
1: 68 percent / TsOH / benzene / 4 h
2: 3-chloroperbenzoic acid / CH2Cl2 / 15 h / 0 - 20 °C
View Scheme
参考文献
Efange, Simon M. N.; Kamath, Ashok P.; Khare, Anil B.; Kung, Mei-Ping; Mach, Robert H.; Parsons, Stanley M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 24 p. 3905 - 3914