二氯(1,10-亚铁试剂)钯(II)合成路线 （共 30 条）
反应条件
in tetrahydrofuran react. PdCl(CONC5H11)(phen) with N-chlorosuccinimide in THF;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in tetrahydrofuran react. PdCl(CONHC3H7)(phen) and CuCl2 in THF;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in tetrahydrofuran react. PdCl(CONHC4H9)(phen) and CuCl2 in THF;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in tetrahydrofuran react. PdCl(CONHC5H11)(phen) and CuCl2 in THF;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in tetrahydrofuran react. PdCl(CON(CH2)4O)(phen) and CuCl2 in THF;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in neat (no solvent) Kinetics; thermal decompn. at 220 °C (investigated by thermogravimetry);; detected by UV-spectroscopy, sepn. by dissolving (Ni(C12H8N2)2Cl2) in ethanol and crystn. from alc. soln. on removal of solvent;;
参考文献
Thermochimica Acta, , vol. 177, p. 93 - 100
反应条件
in chloroform-d1 byproducts: PPh(C6H4Cl-2)2; NMR tube was charged with Pd-complex and ligand in CDCl3, heated to 90°C for 1 h;
参考文献
Inorganica Chimica Acta, , vol. 342, p. 236 - 240
反应条件
1: acetonitrile 2: hexane View Scheme
参考文献
Aresta, Michele; Giannoccaro, Potenzo; Tommasi, Immacolata; Dibenedetto, Angela; Lanfredi, Anna Maria Manotti; Ugozzoli, Franco
Organometallics, 2000 , vol. 19, # 19 p. 3879 - 3889
反应条件
in acetonitrile to suspn. PdCl2(phen) in CH3CN was added piperidine (1:2), suspn. was allowed to react under stirring with CO (0.1 MPa) at 313 K for 3 h; filtered off, washed with CH3CN/CH3OH (10:1), and dried in vacuo; elem.anal.;
参考文献
Aresta, Michele; Giannoccaro, Potenzo; Tommasi, Immacolata; Dibenedetto, Angela; Lanfredi, Anna Maria Manotti; Ugozzoli, Franco
Organometallics, 2000 , vol. 19, # 19 p. 3879 - 3889
反应条件
in acetonitrile to suspn. PdCl2(phen) in MeCN was added piperidine (1:10), mixt. was reacted with CO (0.1 MPa) at room temp. for 4 h; mixt. was concd. and filtered; elem. anal.;
参考文献
Aresta, Michele; Giannoccaro, Potenzo; Tommasi, Immacolata; Dibenedetto, Angela; Lanfredi, Anna Maria Manotti; Ugozzoli, Franco
Organometallics, 2000 , vol. 19, # 19 p. 3879 - 3889
