in neat (no solvent, solid phase) byproducts: NaCl; placing of CuCl2 and NaS2CNEt2 in 1:2 ratio to the reactor; sealing, vibrating for 60 min; sublimating in vac. at 180-190°C; crystn.; elem. anal.;
参考文献
Petrova; Makhaev
Russian Journal of Inorganic Chemistry, 2007 , vol. 52, # 6 p. 865 - 870
in neat (no solvent, solid phase) byproducts: NaCl; placing of CdCl2 and NaS2CNEt2 in 1:2 ratio to the reactor; sealing, vibrating for 60 min; sublimating in vac. at 180-230°C; crystn.; elem. anal.;
参考文献
Petrova; Makhaev
Russian Journal of Inorganic Chemistry, 2007 , vol. 52, # 6 p. 865 - 870
in ethanol byproducts: NaCl; stoich. amts. of FeCl3*6H2O and Na diethyldithiocarbamate in EtOH; filtered; ppt. washed with water and EtOH; dried at room temp.;
in methanol (N2); refluxing a suspn. of ruthenium complex and ligand in MeOH for 10 h; filtration, washing with methanol, ether, drying in vac., recrystn. (CH2Cl2/hexane, 0°C, 1 h); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 689, # 11 p. 1978 - 1990
