water in further solvent(s) byproducts: C6H5Cl; Sonication; (N2); solvent = 1,1,3,3-tetramethylurea contg. water; 2 equivs. of Zn powder used; 30 °C, ultrasound applied for 8 h; 100percent conversion; not isolated; conversion and yield detd. by quenching with I2;