2,7-二甲基-1,8-萘啶合成路线 （共 10 条）
反应条件
potassium hydroxide; hydrogen; Lindlar's catalyst in methanol Hydrogenation; P=3040 Torr; 5 h;
参考文献
He, Chuan; Lippard, Stephen J
Tetrahedron, 2000 , vol. 56, # 42 p. 8245 - 8252
反应条件
potassium hydroxide; hydrogen; Lindlar's catalyst in methanol
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.; Tzimos, Vasilios
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1017 - 1019
反应条件
1: in water 3 h; cooling; 2: With sulfuric acid; nitrobenzene T=110°C; Skraup synthesis; 0.5 h; 3: With sodium hydroxide in water pH=10; 1 h; cooling;
参考文献
Vu, Choua; Walker, DeeDee; Wells, Jason; Fox, Stephen
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 4 p. 829 - 832
反应条件
1: 60 percent / polyphosphoric acid / 1.25 h / 100 °C 2: 75 percent / paraffin / 0.5 h / 350 °C 3: 92 percent / 2.5percent KOH, H2 / 5percent Pd on CaCO3 / methanol View Scheme
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.; Tzimos, Vasilios
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1017 - 1019
反应条件
1: 75 percent / paraffin / 0.5 h / 350 °C 2: 92 percent / 2.5percent KOH, H2 / 5percent Pd on CaCO3 / methanol View Scheme
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.; Tzimos, Vasilios
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1017 - 1019
反应条件
potassium hydroxide; hydrogen; Lindlar's catalyst Hydrogenation; substitution; P=760 Torr;
参考文献
He, Chuan; Lippard, Stephen J
Tetrahedron, 2000 , vol. 56, # 42 p. 8245 - 8252
反应条件
1: diethyl ether / 1) < -50 deg C, 2) 25 deg C, 2 h 2: KMnO4 / acetone View Scheme
参考文献
Newkome, George R.; Theriot, Kevin J.; Majestic, Veronica K.; Spruell, Perri Anne; Baker, Gregory R.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2838 - 2842
反应条件
1: 1.) NaH / 1.) DMF, 2.) DMF, 120 deg C 2: 70 percent / 70percent aq. H2SO4 / 1.5 h / 120 °C View Scheme
参考文献
Mastalarz, H.; Rulko, F.
Polish Journal of Chemistry, 1994 , vol. 68, # 3 p. 459 - 466
反应条件
sulfolane; triphenylphosphine T=151°C; Rate constant;
参考文献
Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 1 p. 163 - 170
反应条件
selenium(IV) oxide in 1,4-dioxane
0.2 h; Heatingmicrowave;
参考文献
Goswami, Shyamaprosad; Adak, Avijit Kumar
Synthetic Communications, 2003 , vol. 33, # 3 p. 475 - 480
