4-氰基吡啶 N-氧化物合成路线 （共 31 条）
反应条件
sodium hydroxide; trichlorophosphate in n-heptane
参考文献
Marcantonio, Karen; Frey, Lisa; Frantz, Doug; Murry, Jerry A.; Tillyer, Richard
Patent: US2003/55255 A1, 2003 ;
反应条件
trichlorophosphate T=100°C; 24 h;
参考文献
Frey, Lisa F; Marcantonio, Karen; Frantz, Doug E; Murry, Jerry A; Tillyer, Richard D; Grabowski, Edward J.J; Reider, Paul J
Tetrahedron Letters, 2001 , vol. 42, # 39 p. 6815 - 6818
参考文献
Sterling Winthrop Inc.
Patent: US5294612 A1, 1994 ;
反应条件
nanoferrite-[Ru(OH)x] in water T=130°C; 0.5 h; Sealed tubeMicrowave irradiation;
参考文献
Nasir Baig; Varma, Rajender S.
Green Chemistry, 2013 , vol. 15, # 2 p. 398 - 417
反应条件
copper acetylacetonate; potassium tert-butylate; oxygen in toluene T=110°C; 2 h;
参考文献
Shen, Yan; Chen, Jiuxi; Liu, Miaochang; Ding, Jinchang; Gao, Wenxia; Huang, Xiaobo; Wu, Huayue
Chemical Communications, 2014 , vol. 50, # 33 p. 4292 - 4295
反应条件
1: CH2Cl2 / 1.5 h / Ambient temperature 2: aq. (NH4)2S2O8 / 1 h / Heating View Scheme
参考文献
Katz, R B; Mistry, J; Mitchell, M B
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 317 - 326
反应条件
trifluoroacetic anhydride T=120°C; 144 h;
参考文献
Wang, Li-Hsing; Zipse, Hendrik
Liebigs Annales, 1996 , # 10 p. 1501 - 1509
反应条件
1: 65 percent / phosphorus oxychloride; phosphorus pentachloride / 3 h / 120 - 130 °C 2: 65 percent / sodium hydride / dimethylformamide / 4 h / 20 °C 3: 56 percent / H2; NH3 / palladium on charcoal / ethanol / 8 h / 45 °C / 2280 Torr View Scheme
参考文献
Leroy; Bigan; Blondeau
Synthetic Communications, 1997 , vol. 27, # 17 p. 2905 - 2916
反应条件
titanium tetrachloride; tin(ll) chloride in diethyl ether 0.5 h; Ambient temperature;
参考文献
Balicki, Roman; Kaczmarek, Lukasz; Malinowski, Marek
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 897 - 900
反应条件
in acetonitrile T=81°C; 4 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 2 p. 487 - 489
