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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-乙酰基苯硼酸
合成路线
（共 161 条）
149104-90-5
4-乙酰基苯硼酸
→
反应条件
123-31-9
对苯二酚
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
149104-90-5
4-乙酰基苯硼酸
→
反应条件
3233-32-7
4-乙酰氧基苯酚
+
123-31-9
对苯二酚
反应条件
1: phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca, M446G mutant; NADPH / dimethyl sulfoxide / 30 °C / Tris/HCl buffer; Enzymatic reaction 2: phosphite dehydrogenase; 4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; NADPH / dimethyl sulfoxide / 24 °C / Tris/HCl buffer; Enzymatic reaction View Scheme
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
106-38-7
对溴甲苯
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
反应条件
lithium niobate; palladium diacetate; potassium carbonate in ethanol; water; paraffin oil T=87 - 88°C; Suzuki Coupling; 0.5 h;
参考文献
Ultrasonics Sonochemistry, , vol. 21, # 4 p. 1305 - 1309
762-04-9
亚磷酸二乙酯
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
25944-71-2
(4-乙酰基苯基)-磷酸二乙酯
反应条件
copper(I) oxide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; 24 h;
参考文献
Zhuang, Rongqiang; Xu, Jian; Cai, Zhenshi; Tang, Guo; Fang, Meijuan; Zhao, Yufen
Organic Letters, 2011 , vol. 13, # 8 p. 2110 - 2113
22445-41-6
1,3-二甲基-5-碘苯
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
25570-02-9
3,3',5,5'-四甲基联苯
+
677022-27-4
反应条件
C34H38Cl2N4Pd; caesium carbonate in 1,4-dioxane T=100°C; Suzuki coupling; 25 h;
参考文献
Morgan, Brad P.; Galdamez, Gabriela A.; Gilliard Jr., Robert J.; Smith, Rhett C.
Dalton Transactions, 2009 , # 11 p. 2020 - 2028
201230-82-2
+
100-44-7
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
782-92-3
+
6420-94-6
反应条件
potassium phosphate; palladium diacetate; tri-cyclo-hexyl-phosphine in water T=80°C; Suzuki carbonylation; P=7500.75 Torr; 20 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Tetrahedron Letters, 2010 , vol. 51, # 47 p. 6146 - 6149
591-50-4
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
92-91-1
反应条件
potassium carbonate in ethanol T=80°C; Suzuki-Miyaura coupling; 12 h; Inert atmosphere;
参考文献
Li, Liuyi; Wang, Jinyun; Wu, Tao; Wang, Ruihu
Chemistry - A European Journal, 2012 , vol. 18, # 25 p. 7842 - 7851
108-86-1
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
92-91-1
反应条件
tri-tert-butyl phosphine; palladium diacetate; potassium hydroxide in tetrahydrofuran; water T=24°C; Suzuki-Miyaura Coupling; 0.0833333 h; Flow reactor;
参考文献
Nagaki, Aiichiro; Takabayashi, Naofumi; Moriwaki, Yuya; Yoshida, Jun-Ichi
Chemistry - A European Journal, 2012 , vol. 18, # 38 p. 11871 - 11875
100-63-0
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
92-91-1
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water T=60°C; Suzuki Coupling;
参考文献
Liu, Jin-Biao; Zhou, He-Ping; Peng, Yi-Yuan
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2872 - 2875
108-90-7
+
149104-90-5
4-乙酰基苯硼酸
→
反应条件
92-91-1
反应条件
palladium diacetate; caesium carbonate; P-phenyl-2,2,6,6-tetramethyl-phosphorinan-4-ol in toluene T=110°C; Suzuki-Miyaura cross coupling; 12 h; Inert atmosphere;
参考文献
Ullah, Ehsan; McNulty, James; Larichev, Vladimir; Robertson, Al J.
European Journal of Organic Chemistry, 2010 , # 35 p. 6824 - 6830
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