2,5-二溴-3-辛基噻吩合成路线 （共 7 条）
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=0°C; 72 h; Darkness;
参考文献
Dilien, Hanne; Palmaerts, Arne; Lenes, Martijn; De Boer, Bert; Blom, Paul; Cleij, Thomas J.; Lutsen, Laurence; Vanderzande, Dirk
Macromolecules, 2010 , vol. 43, # 24 p. 10231 - 10240
反应条件
in N-methyl-acetamide; pyrrolidin-1-yl-2,5-dione
参考文献
ADVENT TECHNOLOGIES, S.A.
Patent: US2011/82261 A1, 2011 ;
反应条件
1: [1,3-bis(diphenylphosphino) propane] dichloronickel(II) 2: N-bromosuccinmide / N,N-dimethyl-formamide / 72 h / 0 °C / Darkness View Scheme
参考文献
Macromolecules, , vol. 43, # 24 p. 10231 - 10240
反应条件
N-bromosuccinmide Multistep reaction;
参考文献
Journal de Chimie Physique et de Physico-Chimie Biologique, , vol. 95, # 6 p. 1180 - 1183
反应条件
1: 2,3-dihydro-thieno[3,4-b][1,4]dioxine With n-butyllithium in tetrahydrofuran T=-78 - 0°C; 2 h; 2: With magnesium; ethylene dibromide in tetrahydrofuran T=0°C; 1 h; 3: 2,5-dibromo-3-octadecylthiophene With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; 36 h;
参考文献
Pepitone, Michael F.; Eaiprasertsak, Kalya; Hardaker, Stephen S.; Gregory, Richard V.
Organic Letters, 2003 , vol. 5, # 18 p. 3229 - 3232
反应条件
bis(1,3-diphenylphosphinopropane) nickel(II) chloride
参考文献
Buvat; Hourquebie
Journal de Chimie Physique et de Physico-Chimie Biologique, 1998 , vol. 95, # 6 p. 1180 - 1183
参考文献
ADVENT TECHNOLOGIES, S.A.
Patent: US2011/82261 A1, 2011 ;
