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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯酚
合成路线
（共 1374 条）
25236-64-0
2,2,2-三氟乙基甲磺酸酯
+
150-76-5
4-甲氧基苯酚
→
反应条件
62158-88-7
+
19013-30-0
4-甲氧基苯基甲磺酸
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=140°C; 20 h; Title compound not separated from byproducts;
参考文献
Camps, F.; Coll, J.; Messeguer, A.; Pericas, M, A.
Synthesis, 1980 , # 9 p. 727 - 728
75-89-8
2,2,2-三氟乙醇
+
150-76-5
4-甲氧基苯酚
+
71-43-2
苯
→
反应条件
62158-88-7
+
613-37-6
4-甲氧基联苯
反应条件
1: 4-methoxy-phenol With nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile 0.25 h; 2: 2,2,2-trifluoroethanol; benzene With caesium carbonate; acetone in acetonitrile 24 h; Inert atmosphereUV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
75-89-8
2,2,2-三氟乙醇
+
150-76-5
4-甲氧基苯酚
+
762-72-1
烯丙基三甲基硅烷
→
反应条件
140-67-0
4-烯丙基苯甲醚
+
62158-88-7
反应条件
1: 4-methoxy-phenol With nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile 0.25 h; 2: 2,2,2-trifluoroethanol; allyl-trimethyl-silane With caesium carbonate; acetone in acetonitrile 24 h; Inert atmosphereUV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
591-80-0
+
75-89-8
2,2,2-三氟乙醇
+
150-76-5
4-甲氧基苯酚
→
反应条件
24962-83-2
+
62158-88-7
+
100-66-3
反应条件
1: 4-methoxy-phenol With nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile 0.25 h; 2: 3-vinylpropionic acid; 2,2,2-trifluoroethanol With caesium carbonate; acetone in acetonitrile 24 h; Inert atmosphereUV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
57389-70-5
+
150-76-5
4-甲氧基苯酚
→
反应条件
62247-92-1
反应条件
sodium hydroxide
参考文献
Leistner,S.; Wagner,G.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1976 , vol. 16, p. 482
150-76-5
4-甲氧基苯酚
→
反应条件
62248-41-3
反应条件
1: sodium hydride / N,N-dimethyl-formamide / 20 - 80 °C / Inert atmosphere 2: hydrogen bromide / 4 h / Inert atmosphere; Reflux 3: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux View Scheme
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
150-76-5
4-甲氧基苯酚
→
反应条件
62248-42-4
反应条件
1: sodium hydride / N,N-dimethyl-formamide / 20 - 80 °C / Inert atmosphere 2: hydrogen bromide / 4 h / Inert atmosphere; Reflux 3: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux View Scheme
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
150-76-5
4-甲氧基苯酚
+
536-74-3
→
反应条件
62594-98-3
反应条件
Fe-Al-MCM-41 in cyclohexane T=80°C; 2 h;
参考文献
Haldar, Satyajit; Koner, Subratanath
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 49 - 55
150-76-5
4-甲氧基苯酚
+
536-74-3
→
反应条件
62594-98-3
反应条件
potassium hydroxide; tributyl-amine; tin(IV) chloride 1) C6H5Cl, 60 deg C, 30 min, 2) C6H5Cl, EtOH, H2O, reflux, 1 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Yamaguchi, Masahiko; Arisawa, Mieko; Omata, Kenji; Kabuto, Kuninobu; Hirama, Masahiro; Uchimaru, Tadafumi
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7298 - 7305
150-76-5
4-甲氧基苯酚
+
109-64-8
→
反应条件
6267-37-4
反应条件
sodium hydroxide 4 h; Heating;
参考文献
Carbonara, Giuseppe; Fracchiolla, Giuseppe; Loiodice, Fulvio; Tortorella, Paolo; Conte-Camerino, Diana; De Luca, Annamaria; Liantonio, Antonella
Farmaco, 2001 , vol. 56, # 10 p. 749 - 754
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