反应条件
1.1: potassium carbonate / acetonitrile / 20 °C / Reflux 2.1: 16 h / 200 °C / Inert atmosphere 3.1: potassium carbonate / acetone / 6 h / Reflux 4.1: 9-borabicyclo-[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C 4.2: 6 h / Reflux 5.1: pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve View Scheme
参考文献
UNIVERSITY OF NOTTINGHAM; BAKER, Jillian G.; FISCHER, Peter M.; FROMONT, Christophe; GARDINER, Sheila M.; HILL, Stephen J.; JADHAV, Gopal; KELLAM, Barrie; MISTRY, Shailesh; WOOLARD, Jeanette
Patent: WO2012/104659 A1, 2012 ;
WO 2012/104659 A1