甲基 3-苯基-DL-丙氨酸酯合成路线 (共 43 条)
反应条件
palladium diacetate; p-benozquinone P=760.051 Torr; 6 h; Reflux;
参考文献
Lopez, Blanca; Rodriguez, Aleix; Santos, David; Albert, Joan; Ariza, Xavier; Garcia, Jordi; Granell, Jaume
Chemical Communications, 2011 , vol. 47, # 3 p. 1054 - 1056
反应条件
palladium diacetate; p-benozquinone in acetic acid T=120°C; 6 h; Overall yield = 91 percent;
参考文献
Albert, Joan; Ariza, Xavier; Calvet, Teresa; Font-Bardia, Merce; Garcia, Jordi; Granell, Jaume; Lamela, Andrea; Lopez, Blanca; Martinez, Manuel; Ortega, Laura; Rodriguez, Aleix; Santos, David
Organometallics, 2013 , vol. 32, # 2 p. 649 - 659
反应条件
(+)-(2R,3R,11R,12R)-1,4,7,10,13,16-hexaoxacyclooctadecane-2,3,11,12-tetracarboxylic acid in various solvent(s) T=25°C; pH=2.5; Electrochemical reaction;
参考文献
Salami; Jira; Otto, Hans-Hartwig
Pharmazie, 2005 , vol. 60, # 3 p. 181 - 185
反应条件
Alcalase; water in tert-butyl alcohol T=25°C; kinetic resolution; pH=8.5; 2.5 h; Title compound not separated from byproducts;
参考文献
Chen, Shui-Tein; Wang, Kung-Tsung
Journal of the Chinese Chemical Society, 1999 , vol. 46, # 3 p. 301 - 311
反应条件
Bacillus licheniformis; sodium hydrogencarbonate; BASIONICreg; BC 01 in water; acetonitrile T=30°C; 0.33 h;
参考文献
Zhao, Hua; Jackson, Lee; Song, Zhiyan; Olubajo, Olarongbe
Tetrahedron Asymmetry, 2006 , vol. 17, # 17 p. 2491 - 2498
反应条件
triethylamine in dichloromethane 1 h; Ambient temperature;
参考文献
Kawa, Hajimu; Yamaguchi, Fumihiko; Ishikawa, Nobuo
Chemistry Letters, 1982 , p. 745 - 748
反应条件
potassium carbonate; zinc(II) chloride in tetrahydrofuran T=0°C; 72 h; Inert atmosphereResolution of racemate; enantioselective reaction;
参考文献
Xu, Hao; Tian, Hua; Liu, Qingwen; Wang, Li; Zhang, Suoqin; Zheng, Liangyu
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 5 p. 1108 - 1113,6
反应条件
N,N'-dimethyl-N,N'-propyleneurea T=-20°C; 24 h; Title compound not separated from byproducts;
参考文献
Sabot, Cyrille; Subhash, Pithani V.; Valleix, Alain; Arseniyadis, Stellios; Mioskowski, Charles
Synlett, 2008 , # 2 p. 268 - 272
反应条件
in ethylene glycol dimethyl ether stereoselectivity; Rate constant;
参考文献
Lyubeznova, M. R.; Karpeiskaya, E. I.; Klabunovskii, E. I.; Koreshkov, Yu. D.; Lutsenko, A. I.; Lubuzh, E. D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.1 p. 731 - 737
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 823 - 828