1-苄基-2,3-异亚丙基-rac-甘油合成路线 (共 27 条)
反应条件
sodium hydride in N,N-dimethyl-formamide 15 h; Ambient temperature;
参考文献
Chun, Moon Woo; Shin, Dae Hong; Moon, Hyung Ryong; Lee, Jeewoo; Park, Hokoon; Jeong, Lak Shin
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 11 p. 1475 - 1480
反应条件
potassium hydroxide in toluene 16 h; Heating;
参考文献
Tirosh, Oren; Kohen, Ron; Katzhendler, Jehoshua; Gorodetsky, Raphael; Barenholz, Yechezkel
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 2 p. 383 - 389
反应条件
PMA T=20°C; 0.0333333 h;
参考文献
Zeynizadeh, Behzad; Sadighnia, Leila
Phosphorus, Sulfur and Silicon and the Related Elements, 2008 , vol. 183, # 9 p. 2274 - 2279
参考文献
Sanofi
Patent: US4423071 A1, 1983 ;
反应条件
in toluene T=80°C; 4 h;
参考文献
US2005/58620 A1, ;
Page/Page column 18; 26 ;
反应条件
potassium carbonate T=220°C; 32 h; AutoclaveInert atmosphere; chemoselective reaction;
参考文献
Selva, Maurizio; Benedet, Vanni; Fabris, Massimo
Green Chemistry, 2012 , vol. 14, # 1 p. 188 - 200
反应条件
potassium carbonate T=190°C; 18 h; AutoclaveInert atmosphere; chemoselective reaction;
参考文献
Green Chemistry, , vol. 14, # 1 p. 188 - 200
反应条件
sodium; toluene Erwaermen der erhaltenen Loesung mit Benzylchlorid;
参考文献
Journal of the Chemical Society, , p. 2666
参考文献
DE403050 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1444
反应条件
1: 79 percent / 1.5 N aq. H2SO4 / 2.5 h / Heating 2: 61 percent / KOH / toluene / Heating View Scheme
参考文献
Schott, Herbert; Schwendener, Reto A.
Liebigs Annales, 1996 , # 3 p. 365 - 369