3-苯基-2-丙炔-1-醇合成路线 （共 165 条）
反应条件
manganese(IV) oxide; triazolium salt; 1,8-diazabicyclo[5.4.0]undec-7-ene
T=20°C;
参考文献
Maki, Brooks E.; Chan, Audrey; Phillips, Eric M.; Scheidt, Karl A.
Tetrahedron, 2009 , vol. 65, # 16 p. 3102 - 3109
反应条件
triethylamine in tetrahydrofuran
T=0°C; 0.25 h;
参考文献
Deorazio, Russell Joseph; Nikam, Sham Shridhar; Scott, Ian Leslie; Sherer, Brian Alan; Wise, Lawrence David
Patent: US2003/236286 A1, 2003 ;
Location in patent: Page 19 ;
反应条件
manganese(IV) oxide; sodium cyanide in tetrahydrofuran
T=20°C; 6 h;
参考文献
Foot, Jonathan S.; Kanno, Hisashi; Giblin, Gerard M. P.; Taylor, Richard J. K.
Synthesis, 2003 , # 7 p. 1055 - 1064
反应条件
1: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, RT
2: 13 percent Spectr. / BCl3 / pentane; hexane / 1.) 0 deg C, 15 min, 2.) RT, 2 h
View Scheme
参考文献
Goff, Dane A.; Harris, Ralph N.; Bottaro, Jeffrey C.; Bedford, Clifford D.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4711 - 4714
反应条件
1: 65 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 24 h / 20 °C
2: 28 percent / PtCl4 / dioxane / 0.08 h / 20 °C
View Scheme
参考文献
Pastine, Stefan J.; Youn, So Won; Sames, Dalibor
Organic Letters, 2003 , vol. 5, # 7 p. 1055 - 1058
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
T=20°C; 24 h;
参考文献
Pastine, Stefan J.; Youn, So Won; Sames, Dalibor
Organic Letters, 2003 , vol. 5, # 7 p. 1055 - 1058
反应条件
1: H2 / 5percent Pd/BaSO4 / pyridine
View Scheme
参考文献
Goering, Harlan L.; Kantner, Steven S.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 721 - 724
反应条件
1: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate
T=0°C;
2: With ozone
参考文献
Molinaro, Carmela; Jamison, Timothy F.
Journal of the American Chemical Society, 2003 , vol. 125, # 27 p. 8076 - 8077
参考文献
Duboudin,J.G.; Jousseaume,B.
Journal of Organometallic Chemistry, 1979 , vol. 168, p. 1 - 11
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Hazra, Chinmoy K.; Oestreich, Martin
Organic Letters, 2012 , vol. 14, # 15 p. 4010 - 4013
