3-苯基-2-丙炔-1-醇合成路线 (共 165 条)
参考文献
Tetrahedron Letters, , vol. 37, # 50 p. 9059 - 9062
反应条件
1: With diethylzinc; triphenylphosphine in hexane; dichloromethane T=20°C; 4 h; Inert atmosphere; 2: With hydrogenchloride; water in hexane; dichloromethane
参考文献
Wilson, Erin E.; Oliver, Allen G.; Hughes, Russell P.; Ashfeld, Brandon L.
Organometallics, 2011 , vol. 30, # 19 p. 5214 - 5221
反应条件
sulfuric acid in methanol
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2173 - 2176
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the American Chemical Society, , vol. 83, p. 1968 - 1974
反应条件
water in acetone T=50°C; 96 h; Product distribution;
参考文献
Hanack, Michael; Massa, Friedrich Wilhelm
Tetrahedron Letters, 1981 , vol. 22, p. 557 - 558
反应条件
diethyl ether; nitrogen
参考文献
Journal of the American Chemical Society, , vol. 47, p. 862
反应条件
sodium hydroxide; water in acetone Combinatorial reaction / High throughput screening (HTS);
参考文献
US2007/43234 A1, ;
Page/Page column 58 ;
反应条件
1: 1 N aq. HCl / CH2Cl2 2: diisobutylaluminum hydride / tetrahydrofuran; hexane / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 16 p. 3662 - 3668
反应条件
1: 1.) AlCl3, 3.) triethylamine, NaHCO3 2: 1 N aq. HCl / CH2Cl2 3: diisobutylaluminum hydride / tetrahydrofuran; hexane / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 16 p. 3662 - 3668
反应条件
1: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 0.5 h; 2: With sodium tetrahydroborate; water in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Synthesis, , # 9 art. no. M12811SS, p. 1375 - 1382