3-苯基-2-丙炔-1-醇合成路线 （共 165 条）
反应条件
1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 3 h / 0 °C / |Darkness 2: diethylzinc; oxygen / dichloromethane; n-heptane / 14 h / 20 °C / |Darkness View Scheme
参考文献
Jammi, Suribabu; Mouysset, Dominique; Siri, Didier; Bertrand, Michele P.; Feray, Laurence
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1589 - 1603
反应条件
dicobalt octacarbonyl; ammonium cerium(IV) nitrate; dimethylsulfide borane complex; trifluoroacetic acid Yield given. Multistep reaction;
参考文献
McComsey, David F.; Reitz, Allen B.; Maryanoff, Cynthia A.; Maryanoff, Bruce E.
Synthetic Communications, 1986 , vol. 16, # 12 p. 1535 - 1550
反应条件
TBBDA T=20°C; 0.2 h; Neat (no solvent);
参考文献
Ghorbani-Vaghei; Akbari-Dadamahaleh; Amiri
Journal of the Iranian Chemical Society, 2010 , vol. 7, # 2 p. 301 - 307
反应条件
1: LiAlH4 / tetrahydrofuran / 3 h / Heating 2: Et3N / benzene / 1 h / 25 - 30 °C View Scheme
参考文献
Tomassy, Beata; Zwierzak, Andrzej
Synthetic Communications, 1998 , vol. 28, # 7 p. 1201 - 1214
反应条件
manganese(IV) oxide; ammonia; magnesium sulfate in tetrahydrofuran; isopropyl alcohol T=20°C; 2 h;
参考文献
McAllister, Graeme D.; Wilfred, Cecilia D.; Taylor, Richard J. K.
Synlett, 2002 , # 8 p. 1291 - 1292
反应条件
1: H2, quinoline / Lindlar catalyst / ethyl acetate / 0.25 h / 103.4 - 258.6 Torr 2: pyridine, MeSO2Cl / CH2Cl2 / 18 h / 5 °C View Scheme
参考文献
Davis, Franklin A.; Reddy, R. Thimma
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2599 - 2606
反应条件
1: 98 percent / Et3N / CH2Cl2 / 2 h / 0 °C 2: 88 percent / tributylcetylphosphonium bromide / toluene / 4 h / 60 °C 3: Ni<P(OPh)3> / 18 h / 120 °C 4: 98 percent / H2 / 10percent Pd/CaCO3 / ethyl acetate / 6 h / 70 °C / 7757.2 Torr 5: 90 percent / 30percent aq. HCl / 14 h / Heating View Scheme
参考文献
Jackson, W. Roy; Perlmutter, Patrick; Smallridge, Andrew J.
Australian Journal of Chemistry, 1988 , vol. 41, # 8 p. 1201 - 1208
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite in acetonitrile T=35°C; pH 6.7;
参考文献
Journal of Organic Chemistry, , vol. 64, # 7 p. 2564 - 2566
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=20°C; 12 h;
参考文献
Wessig, Pablo; Mueller, Gunnar
Chemical Communications, 2006 , # 43 p. 4524 - 4526
反应条件
1: 92 percent / PBr3; pyridine / diethyl ether / 3.5 h / -40 - 20 °C 2: 60 percent / K2CO3 / acetonitrile / 12 h / 20 °C View Scheme
参考文献
Fuji, Koji; Morimoto, Tsumoru; Tsutsumi, Ken; Kakiuchi, Kiyomi
Chemical Communications, 2005 , # 26 p. 3295 - 3297
